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1 article(s) from Yoshida, Keisuke

Asymmetric desymmetrization of meso-diols by C₂-symmetric chiral 4-pyrrolidinopyridines

Hartmut Schedel,
Keizo Kan,
Yoshihiro Ueda,
Kenji Mishiro,
Keisuke Yoshida,
Takumi Furuta and
Takeo Kawabata

Beilstein J. Org. Chem. 2012, 8, 1778–1787, doi:10.3762/bjoc.8.203

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Graphical Abstract

Figure 1: Chiral PPY catalysts.

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Scheme 1: Asymmetric desymmetrization of 5 with catalyst 3.

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Scheme 2: Preparation of a small library of chiral C₂-symmetric PPY catalysts (reference, see [12]).

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Scheme 3: Amplification of enantiomeric purity of the major enantiomer produced at the step of asymmetric des...

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Scheme 4: Acylative kinetic resolution of racemic-6 with catalyst 12b.

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Figure 2: A hypothetical model for the transition-state assembly of the asymmetric acylation of 5 promoted by...

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Figure 3: An alternative model for the transition state assembly of the asymmetric acylation of 5 promoted by...

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Published 17 Oct 2012

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Asymmetric desymmetrization of meso-diols by C2-symmetric chiral 4-pyrrolidinopyridines

Asymmetric desymmetrization of meso-diols by C₂-symmetric chiral 4-pyrrolidinopyridines